variavel0=Farith M. Absi Salas - farith@lttc.coppe.ufrj.br PEM/COPPE/UFRJ Alexandre P. Oliveira - alexandre@lttc.coppe.ufrj.br PEM/COPPE/UFRJ Daniela V.F.M. Rey Silva - daniela@lttc.coppe.ufrj.br PEM/COPPE/UFRJ Helcio R. B. Orlande - helcio@serv.com.ufrj.br COPPE/UFRJ Abstract. This paper deals with the estimation of the thermal conductivity and of the volumetric heat capacity of solids. The experimental setup designed in our previous works consists of a heater symmetrically assembled between two pieces of the specimen with unknown properties. Transient temperature measurements taken in the heated surface of the specimen are used in two estimation procedures, namely: the Levenberg-Marquardt Method and the Sequential Parameter Estimation Technique. Results are presented for the estimation of the properties of Teflon. Keywords. Thermal Conductivity, Volumetric Heat Capacity, Parameter Estimation, Levenberg-Marquardt, Sequential Parameter Estimation.